2,3-Dichloronitrobenzene → HCID 15077491, compound

HRID 1074192Notes

Reaction equation

HRID 1074192 reaction equation
Cl[C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[SH:12][C:13]1[N:14]([CH3:18])[CH:15]=[CH:16][N:17]=1>>[Cl:8][C:7]1[CH:6]=[CH:5][CH:4]=[C:3]([N+:9]([O-:11])=[O:10])[C:2]=1[S:12][C:13]1[N:14]([CH3:18])[CH:15]=[CH:16][N:17]=1

Participants

3

Reactant 2

HCID 185552,3-DichloronitrobenzeneHCID 178480602HCID 178480602, compound

Product 1

HCID 15077491HCID 15077491, compoundYield 74.2%

Procedure

Starting with 1.92 g (10 mmoles) of 2,3-dichloronitrobenzene and 1.14 g (10 mmoles) of 2-mercapto-1-methylimidazole and following the procedure described in Example 1 there was obtained 2 g (74%) of the product as yellow prisms, mp 102°-104° C.

Sources & evidence

ORD record
ord-9e06c47069d044d9af37d9ecc60507c7
Source dataset
uspto-grants-1990_11
Patent number
US04973599

Reaction notes

Loading…