HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → Benzyl 4-Hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium 4-hydroxybenzoate | HCID 16219477 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzyl 4-Hydroxybenzoate | HCID 7180 | 74% |
Reaction Steps
Sodium p-hydroxybenzoate (64 g) and 51 g of benzyl chloride were added to 150 g of dimethylformamide, and reacted at 100° C. for 3 hours. Benzyl p-hydroxybenzoate was obtained in a yield of 74%. The ratio of benzyl p-benzyloxybenzoate, a by-product, formed was 10%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04973737 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-8ad97fb84fbe49b499868575a5da03c6 |
| Source note | uspto-grants-1990_11 |