HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,6-dimethoxy-1,3,5-triazine → HCID 20496349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,6-dimethoxy-1,3,5-triazine | HCID 27840 | — |
| Reactant | Benzo[b]thiophene-3-sulfonyl isocyanate | HCID 13178325 | — |
| Product | HCID 20496349 | HCID 20496349 | 85.7% |
Reaction Steps
Using the procedure of Example 3, and substituting 1.6 g of 2-amino-4,6-dimethoxy-1,3,5-triazine and 2.4 g of benzothiophene-3-sulfonyl isocyanate, a yield of 3.4 g of the desired product was obtained melting at 152°. It showed absorption peaks by Nuclear Magnetic Resonance (60 MC) at; 3.95 δ (CH3O), 7-8 δ (benzohydrogens) and 8.3 δ (thiophene hydrogen) consistent for the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04391627 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-256aa53b3a874ff0af9b4de42015cfc9 |
| Source note | uspto-grants-1983_07 |