HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinyl alcohol → Polyethylene glycol monolaurate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinyl alcohol | HCID 11199 | — |
| Reactant | N-octadecyl-D-gluconamide | HCID 87614 | — |
| Reactant | Span(R) 20 | HCID 16218599 | — |
| Product | Polyethylene glycol monolaurate | HCID 62699 | — |
Reaction Steps
Comparative experiments were carried out in which in place of N-octadecyl gluconamide, the suspension stabilizers Gohsenol KP 08, Armotan® MP (sorbitan monopalmitate), Armotan® ML (sorbitan monolaurate) Tween® 20 (polyoxyethylene (20) monolaurate) and Tween® 21 (polyoxyethylene (4) monolaurate) were used. Only the results obtained with Tween® 21 (polyoxyethylene (4) monolaurate) compared with those obtained with N-octadecyl gluconamide. When only Gohsenol KP 08 was used, the results obtained were distinctly poorer. In all other cases destabilization of the suspension was observed after 1 to 2 hours polymerization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04391962 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-81417b9f42044341874ff615b205f129 |
| Source note | uspto-grants-1983_07 |