2,6-Di-tert-butyl-4-methylphenol → HCID 54180297, compound

HRID 1074524Notes

Reaction equation

HRID 1074524 reaction equation
[B:1](OC1CCC(C)C(C)C1)([O:11][CH:12]1[CH2:17][CH2:16][CH:15]([CH3:18])[CH:14]([CH3:19])[CH2:13]1)[O:2][CH:3]1[CH2:8][CH2:7][CH:6]([CH3:9])[CH:5]([CH3:10])[CH2:4]1.[C:29]([C:33]1[CH:38]=[C:37]([CH3:39])[CH:36]=[C:35]([C:40]([CH3:43])([CH3:42])[CH3:41])[C:34]=1[OH:44])([CH3:32])([CH3:31])[CH3:30]>>[B:1]([O:44][C:34]1[C:33]([C:29]([CH3:32])([CH3:31])[CH3:30])=[CH:38][C:37]([CH3:39])=[CH:36][C:35]=1[C:40]([CH3:43])([CH3:42])[CH3:41])([O:11][CH:12]1[CH2:17][CH2:16][CH:15]([CH3:18])[CH:14]([CH3:19])[CH2:13]1)[O:2][CH:3]1[CH2:8][CH2:7][CH:6]([CH3:9])[CH:5]([CH3:10])[CH2:4]1

Participants

3

Reactant 2

HCID 314042,6-Di-tert-butyl-4-methylphenolHCID 53894520HCID 53894520, compound

Product 1

HCID 54180297HCID 54180297, compound

Procedure

Bis(3,4-dimethylcyclohexyl) 2,6-di-t-butyl-4-methylphenyl borate was prepared by transesterification of tri(3,4-dimethylcyclohexyl) borate (1.5 mole) with 2,6-di-t-butyl-4-methylphenol (0.5 mole). The reaction mixture was slowly distilled to remove 3,4-dimethylcyclohexanol and the product was obtained as a viscous oil.

Workup

  1. distillationThe reaction mixture was slowly distilled
  2. customto remove 3,4-dimethylcyclohexanol
  3. customthe product was obtained as a viscous oil

Sources & evidence

ORD record
ord-ee97219e3ac64152986f22d5d8516178
Source dataset
uspto-grants-1983_07
Patent number
US04392973

Reaction notes

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