Calcium Hydroxide → HCID 13755316, compound

Participants

Reaction Conditions

Reaction Steps

14.1 g of alpha-chloro-beta-aminopropionitrile hydrochloride was dissolved in 160 g of water, and with stirring, 12 g of calcium hydroxide was gradually added. Then, the reaction mixture was heated to 60° C., and reacted at 60° to 65° C. for 8 hours. After the reaction, the excess of calcium hydroxide was removed by filtration. The residue was analyzed by high-speed liquid chromatography in the same way as in Example 1. The yield of calcium aziridine-2-carboxylate formed was 92.5%.

Provenance & Evidence