HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylbenzene → Prop-2-enenitrile--ethenylbenzene (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylbenzene | HCID 7500 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Catalyst | tert-Butyl peroxybenzoate | HCID 11966 | — |
| Product | Prop-2-enenitrile--ethenylbenzene (1/1) | HCID 62696 | — |
Reaction Conditions
| Temperature | 110 °C |
|---|
Reaction Steps
A mixture of 73 parts styrene and 27 parts acrylonitrile is continuously fed to a stirred polymerization reactor. 50 parts of ethylbenzene are also added as a diluent along with 0.5 parts tert-butyl perbenzoate catalyst. The reaction mixture is heated to 110° C., and the monomers are polymerized by continuous mass polymerization until the initial continuous monomer phase is inverted to form a continuous styrene-acrylonitrile copolymer matrix with residual monomer dispersed throughout the matrix.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04393171 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-ead08b26ccfe4b93899515f52ebaaef5 |
| Source note | uspto-grants-1983_07 |