HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → N-Benzyl-2-cyano-3-(dimethylamino)prop-2-enamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | N-benzyl-2-cyanoacetamide | HCID 668298 | — |
| Product | N-Benzyl-2-cyano-3-(dimethylamino)prop-2-enamide | HCID 54269477 | — |
Reaction Steps
As for Example 1, N-benzyl-2-cyanoacetamide, m.p. 122°-123° C., is heated with N,N-dimethylformamide dimethylacetal to give N-benzyl-2-cyano-3-dimethylaminoacrylamide as colorless needles, m.p. 160.5°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04393217 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-45ec4f7bfe19480b9dd640a68eedd1a9 |
| Source note | uspto-grants-1983_07 |