関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Aluminum Stearate | HCID 12496 | — |
| 反応物 | Aluminum | HCID 5359268 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 反応物 | Sodium brassylate | HCID 11514768 | — |
| 生成物 | Ethylene brassylate | HCID 61014 | 88.1% |
反応手順
Sodium brassylate (0.33 g) and aluminum stearate (1.09 g) were added to 70 g poly(ethylene brassylate) and the mixture heated at 200° C. until a homogeneous viscous mass was obtained. The molar ratio of sodium to aluminum was 2:1. The temperature was then increased to 312° C. and the pressure reduced to 0.3-0.5 mm Hg. The depolymerization reaction was complete in about 3 hours and 88.1% yield ethylene brassylate was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04393223 |
|---|
| 出典データセット | uspto-grants-1983_07 |
|---|
| ORD ID | ord-73818c2acbb44ef5b95ffeada8e92913 |
|---|
| 出典メモ | uspto-grants-1983_07 |
|---|
