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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1074649Erstellt: 25. Oktober 2026

3-Phenoxybenzyl alcohol → 3-Phenoxybenzaldehyde

https://huagongshe.com/reaction/1074649

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Phenoxybenzyl alcoholHCID 26295—
Edukt3-PhenoxybenzaldehydeHCID 38284—
Edukt1-(Dibromomethyl)-3-phenoxybenzeneHCID 104630—
LösungsmittelMethanolHCID 887—
Produkt3-PhenoxybenzaldehydeHCID 38284—
Produkt1-(Bromomethyl)-3-phenoxybenzeneHCID 94544—
Produkt1-(Dibromomethyl)-3-phenoxybenzeneHCID 104630—
ProduktBenzenemethanol, 3-phenoxy-, 1-acetateHCID 170904—

Reaktionsschritte

The resulting m-phenoxybenzyl bromide can be easily esterified in a solvent such as acetic acid to produce m-phenoxybenzyl acetate. The product can be easily converted into m-phenoxybenzyl alcohol by a hydrolysis with a base in a solvent such as methanol. In accordance with the aforementioned treatment, m-phenoxybenzylidene dibromide is converted into m-phenoxybenzaldehyde. Thus, m-phenoxybenzyl acetate and m-phenoxybenzaldehyde are produced by the treatment of the mixture of m-phenoxybenzyl bromide and m-phenoxybenzylidene dibromide, m-phenoxybenzyl acetate and m-phenoxybenzaldehyde can be separated from the mixture by a distillation under a reduced pressure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04393246
Quelldatensatzuspto-grants-1983_07
ORD IDord-00e82e20abc54799aa8446b8cdcb0fdd
Quellennotizuspto-grants-1983_07