HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 53874944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54180953 | HCID 54180953 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53874944 | HCID 53874944 | 89.7% |
Reaction Steps
Ethyl 2-(2-aminothiazol-4-yl)-2-n-octyloxyiminoacetate (syn isomer, 64 g.), 2 N-aqueous solution of sodium hydroxide (196 ml.), methanol (196 ml.) and tetrahydrofuran (300 ml.) were treated in a similar manner to that of Example F-(4) to give 2-(2-aminothiazol-4-yl)-2-n-octyloxyiminoacetic acid (syn isomer, 52.5 g.), mp. 146° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04393059 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-1032880d08534fddaa8b452bc293848d |
| Source note | uspto-grants-1983_07 |