HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 20495230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Catalyst | Copper | HCID 23978 | — |
| Product | HCID 20495230 | HCID 20495230 | — |
Reaction Steps
The diethyl acetal of benzaldehyde (3.6 g) and acetyl chloride (2.5 g) were reacted in the presence of a trace of copper bronze. The product was reacted with 1,2,4-triazole (2.8 g) to give the title compound as a viscous oil which GLC showed to be about 95% pure. Analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04394380 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-04224eff7e094fd3831859ab3df01ff6 |
| Source note | uspto-grants-1983_07 |