化工社化工社 化学情報印刷レポート · 研究参考用
Methylhydroquinone → Methyl-1,4-benzoquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylhydroquinone | HCID 7253 | — |
| 反応物 | Hypochlorite | HCID 61739 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Methyl-1,4-benzoquinone | HCID 11122 | — |
反応手順
2-methyl hydroquinone (1b) of 3.0 g (24 mmol) is dissolved in 150 ml of chloroform, wherein 100 ml each of hypochloride solution which have been so prepared as mentioned above are added and each reaction is made in the same way as described in Example 1, and then 2-methyl benzoquinone (IIb) is obtained. Table below shows the yields of isolation corresponding to each case of the investigation:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04394315 |
| 出典データセット | uspto-grants-1983_07 |
| ORD ID | ord-054885253cbc4b59beba4cc150ab1079 |
| 出典メモ | uspto-grants-1983_07 |