huagongshe.com
HRID1075034

反应详情

EQUATION

反应方程式

HRID 1075034 的结构方程式

REACTANTS

反应物

2
结构：CN(C)Cc1ccc(CSCCN)o1
HCID162203

5-((2-Aminoethyl)thiomethyl)-N,N-dimethyl-2-furanmethanamine

C10H18N2OS

结构：COC1=NS(=O)(=O)N=C1OC
HCID12230538

3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide

C4H6N2O4S

PRODUCTS

生成物

1
结构：COC1=NS(=O)(=O)N=C1NCCSCc1ccc(CN(C)C)o1
HCID178494329

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

2 次

PROCEDURE

实验过程

A solution of 2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethylamine (2.41 g; 11.2 mmoles) [prepared according to the procedure described in Belgian Pat. No. 857,388] in 20 ml of dry methanol was added all at once to a well stirred, cold (8°) suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide (2.0 g; 11.2 mmoles) in 200 ml of methanol. After stirring at 8°-10° for 15 minutes, a methanolic solution of the title compound is produced.

WORKUP

后处理

  1. stirringAfter stirring at 8°-10° for 15 minutes