HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2(1H)-pyrimidinone, 5-chloro-3,4-dihydro-4-thioxo- | HCID 5324558 | — |
| Solvent | Sodium hydride | HCID 24758 | — |
| Product | HCID 178503575 | HCID 178503575 | 21% |
Reaction Steps
5-Chloro-4-thiouracil (0.0027 mol) was dissolved in 1 M sodium hydride (3 ml) and methyl iodide (0.007 mol) added. The solution was stirred at room temperature for 3 hr. and the solid precipitate collected and recrystallised from water; yield 21%, m.p. 254° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395406 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-f0e0bd5863d141bab154410e25b9eb9e |
| Source note | uspto-grants-1983_07 |