HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitro-2-trichloromethylbenzenesulfenyl chloride → HCID 178526732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Reactant | 2-sulfanylpyrimidin-4-ol | HCID 178516529 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178526732 | HCID 178526732 | 94.1% |
Reaction Steps
61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride are reacted with 26.6 g of 4-hydroxy-2-mercaptopyrimidine by a method similar to that described in Example 7. Water is then added and the product is filtered off. 75 g (94% of theory) of 4-hydroxypyrimidin-2-yl-dithio-(4-nitro-2-trichloromethylbenzene), of melting point 174° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395415 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-4e8e2381fd024a3ba9462ebaf3170f4e |
| Source note | uspto-grants-1983_07 |