Dimethyl Sulfate → HCID 20494459, compound

HRID 1075192Notes

Reaction equation

HRID 1075192 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[S:17]([O:22]C)(O[CH3:21])(=[O:19])=[O:18]>>[CH3:1][S:17]([O-:22])(=[O:19])=[O:18].[CH3:21][N+:11]1([CH2:10][CH2:9][CH2:8][CH2:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1

Participants

3

Reactant 2

HCID 6497Dimethyl SulfateHCID 10867725HCID 10867725, compound

Product 1

HCID 20494459HCID 20494459, compound

Procedure

Following the procedure set out in Example 25, N-(4-phenylbutyl)piperidine was reacted with dimethyl sulfate to afford N-methyl-N-(4-phenylbutyl)piperidinium methanesulfonate. M.P. 54°-56° C.

Sources & evidence

ORD record
ord-422af5a7c3774dc38ad7e0dab574b94d
Source dataset
uspto-grants-1983_07
Patent number
US04395410

Reaction notes

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