化工社化工社 化学情報印刷レポート · 研究参考用
2-Octylamine → N-(1-methylheptyl)-4-phenylbutyramide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Octylamine | HCID 12735 | — |
| 反応物 | 4-Phenylbutanoyl Chloride | HCID 11789865 | — |
| 生成物 | N-(1-methylheptyl)-4-phenylbutyramide | HCID 20494534 | — |
反応手順
4-Phenylbutyryl chloride was reacted with 1-methylheptylamine to provide N-(1-methylheptyl)-4-phenylbutyramide, which, when reduced by reaction with dibroane in tetrahydrofuran, provided N-(1-methylheptyl)-4-phenylbutylamine. The amine so formed was reacted with formic acid and formaldehyde to give N-methyl-N-(1-methylheptyl)-4-phenylbutylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04395410 |
| 出典データセット | uspto-grants-1983_07 |
| ORD ID | ord-9265194e26884c63962f648b590441c9 |
| 出典メモ | uspto-grants-1983_07 |