Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | Lauryldimethylamine | HCID 8168 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | HCID 14625834 | HCID 14625834 | — |
Reaction Steps
Into a 1000 mL, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged N,N-dimethyldodecylamine (186.46 grams, 0.875 moles), 1-bromo-2-chloroethane (125.60 grams, 0.875 moles) and methanol (150 mL). The reaction was maintained at 65° C. for 48 hours. Solvent was removed by rotary evaporation under reduced pressure to yield brown oil. The oil was placed in a beaker and stirred with t-butylmethylether (2 L) causing a brownish white precipitate to form. The solids were collected by vacuum filtration. Solids were dried in a vacuum oven at 30° C. overnight Yield 197.0 grams (0.55 moles, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05900475 |
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| Source dataset | uspto-grants-1999_05 |
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| ORD ID | ord-3589b8926cc240f99d954029c2383323 |
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| Source note | uspto-grants-1999_05 |
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