HuagongsheHuagongshe Chemistry Print Report · For research reference only
Manganese sulfate monohydrate → Glucosamine sulfate manganese chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Manganese sulfate monohydrate | HCID 177577 | — |
| Reactant | (3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride | HCID 2723635 | — |
| Solvent | Water | HCID 962 | — |
| Product | Glucosamine sulfate manganese chloride | HCID 86754063 | — |
Reaction Steps
Example 1 was repeated using 450 g of purified water, 107.8 g (0.5 mole) of glucosamine hydrochloride and 42.3 g (0.25 mole) of manganese sulfate monohydrate instead of the sodium sulfate. After freeze drying, glucosamine sulfate manganese chloride was obtained as a white powder in a yield of 144 g (98% of theoretical).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05902801 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-045279f9fee44a129807d5810a9ab026 |
| Source note | uspto-grants-1999_05 |