化工社化工社 化学情報印刷レポート · 研究参考用
1-Methyl-4-piperidone → 5-Methoxy-3-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)pyrrolo[3,2-b]pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Methyl-4-piperidone | HCID 74049 | — |
| 反応物 | 5-methoxy-1H-pyrrolo[3,2-b]pyridine | HCID 5324369 | — |
| 生成物 | 5-Methoxy-3-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)pyrrolo[3,2-b]pyridine | HCID 11010163 | 84% |
反応手順
Beginning with 0.80 gm (5.4 mMol) of 5-methoxypyrrolo-[3,2-b]pyridine and 1.2 mL (10.1 mMol) 1-methyl-4-piperidone, 1.1 gm (84%) of the title compound were recovered as a yellow solid essentially by the procedure described in Example 5. An analytical sample was recrystallized from methanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05905084 |
| 出典データセット | uspto-grants-1999_05 |
| ORD ID | ord-b4ed7dcdb7724f2985fc341b9c4689b3 |
| 出典メモ | uspto-grants-1999_05 |