HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butoxycarbonylalanine → N-[2-(N-tert-Butyloxycarbonyl-L-alanyl-glycyl)-amino-2-deoxy-beta-D-glucopyranosyl]-N-tetradecyl-oleamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butoxycarbonylalanine | HCID 85082 | — |
| Reactant | N-(2-glycyl-amino-2-deoxy-beta-glucopyranosyl)-N-tetradecyl-oleamide | HCID 131721258 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-[2-(N-tert-Butyloxycarbonyl-L-alanyl-glycyl)-amino-2-deoxy-beta-D-glucopyranosyl]-N-tetradecyl-oleamide | HCID 131721257 | 79% |
Reaction Steps
from N-(2-glycyl-amino-2-deoxy-β-glucopyranosyl)-N-tetradecyl-oleamide and N-tert-butyloxycarbonyl-L-alanine. Yield 79%. [α]D =+12.1° (c=0.87, tetrahydrofuran).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05905071 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-fcb97cbe7c024c13bd635435dd9e1ea1 |
| Source note | uspto-grants-1999_05 |