HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15858811, compound → HCID 21309376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15858811 | HCID 15858811 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21309376 | HCID 21309376 | — |
Reaction Steps
(5R,6S)-6-benzyloxycarbonylamino-4-oxa-1-azabicyclo[3,2,0]heptan-7-one (950 mg, 3.624 mmole) was hydrogenated with 3 g of 10% palladium on activated carbon in ethyl acetate (80 ml) at 50 psi hydrogen pressure at room temperature for 6 hrs. after removal of catalyst by filtration, deprotected (5R,6S)-6-amino-4-oxa-1-azabicyclo[3,2,0]heptan-7-one in ethyl acetate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05905076 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-0d6a757672814a92819b2ee952758d81 |
| Source note | uspto-grants-1999_05 |