HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzothiazole → 3-(Prop-2-en-1-yl)-1,3-benzothiazol-3-ium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzothiazole | HCID 7222 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Product | 3-(Prop-2-en-1-yl)-1,3-benzothiazol-3-ium bromide | HCID 177743 | — |
Reaction Steps
135 g of benzothiazole and 121 g of allylbromide were mixed and the mixture was heated for 2 hours on a steam bath to solidify by crystallization. After cooling, diethyl ether was added to wash the crystals. After filtration and drying, the crystals obtained were recrystallized from ethanol. Melting point: 145°-147°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954478 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-bacc7980f0ac48e1bad84dc4e8621280 |
| Source note | uspto-grants-1976_05 |