HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isophthalic Acid → HCID 68140375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isophthalic Acid | HCID 8496 | — |
| Reactant | (1,4-Dioxan-2-yl)methanol | HCID 12655091 | — |
| Catalyst | p-Toluenesulfonic acid | HCID 6101 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 68140375 | HCID 68140375 | 86% |
Reaction Steps
Following the procedure of Example 2, a mixture of 166 grams (1 mole) of isophthalic acid, 295 grams (2.5 moles) of 1,4-dioxanemethanol, 100 milliliters of benzene and 0.1 gram of p-toluenesulfonic acid catalyst gives an 86 percent yield of the white, waxy bis-1,4-dioxanemethanol isophthalate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954742 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-b896f5091ec84ced82669f0712e768b3 |
| Source note | uspto-grants-1976_05 |