Benzene → HCID 86733372, compound

HRID 1075756Notes

Reaction equation

HRID 1075756 reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[O:8]1[CH2:13][CH2:12][O:11][CH2:10][CH:9]1[CH2:14][OH:15].C1C=CC=CC=1>>[C:1]([OH:6])(=[O:7])/[CH:2]=[CH:3]\[C:4]([OH:8])=[O:5].[O:8]1[CH2:13][CH2:12][O:11][CH2:10][CH:9]1[CH2:14][OH:15].[O:8]1[CH2:13][CH2:12][O:11][CH2:10][CH:9]1[CH2:14][OH:15]

Participants

4

Reactant 3

HCID 241BenzeneHCID 7923Maleic AnhydrideHCID 12655091(1,4-Dioxan-2-yl)methanol

Product 1

HCID 86733372HCID 86733372, compoundYield 82%

Procedure

Following the procedure of Example 2, a mixture of 98 grams (1 mole) of maleic anhydride, 354 grams (3.0 moles) of 1,4-dioxanemethanol and 50 milliliters of benzene affords an 82 percent yield of bis-1,4-dioxanemethanol maleate.

Sources & evidence

ORD record
ord-6ef48505d2884ba88fee85264f5eebff
Source dataset
uspto-grants-1976_05
Patent number
US03954742

Reaction notes

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