Toluene → HCID 68139290, compound

Participants

Reaction Steps

Following the procedure of Example 2, a mixture of 87.1 grams (0.5 mole) of sebacic acid, 146.5 grams (1.25 moles) of 1,4-dioxanemethanol, 50 milliliters of toluene and 0.2 gram of dibutyltin dilaurate catalyst yields a waxy product in 87 percent yield which is recrystallized from an isopropanol-water mixture to give the colorless bis-1,4-dioxanemethanol sebacate.

Provenance & Evidence