HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86733377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86733378 | HCID 86733378 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86733377 | HCID 86733377 | 65.6% |
Reaction Steps
0.4 g of sodium hydroxide dissolved in a minimum quantity of water was added to a suspension of 4.8 g pyridine 2.5 -dihydroxybenzenesulphonate dibenzoate in 50 ml of ethanol. The precipitate obtained in the water was recrystallized, and 2.8 g of sodium 2.5-dihydroxybenzenesulphonate dibenzoate were obtained. The infra-red spectrum recorded on a KBr disc, gave maxima at the following frequencies: 1740, 1480, 1465, 1240, 1175, 1060, 1025 and 705 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954767 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-336d74c9a0e6416e9074cc52af0d833c |
| Source note | uspto-grants-1976_05 |