HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-methyl-2H-3-isoquinolone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | N-methyl-2H-3-isoquinolone sulfate | HCID 21541268 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N-methyl-2H-3-isoquinolone | HCID 12435498 | — |
Reaction Steps
70 g. N-methyl-2H-3-isoquinolone sulfate are dissolved, under an atmosphere of nitrogen, in 900 ml. water. 75 g. sodium bicarbonate are added and the mixture is stirred with 500 ml. chloroform. By decantation, there is obtained a chloroform solution of N-methyl-2H-3-isoquinolone, which can be dried over anhydrous sodium sulfate and employed as such or concentrated for a further reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954771 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-c078a18486cf4a12876c27b719da7b99 |
| Source note | uspto-grants-1976_05 |