HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → N-formyl-N-methyl-2-phenyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | N-methyl-2H-3-isoquinolone | HCID 12435498 | — |
| Product | N-formyl-N-methyl-2-phenyl-acetamide | HCID 21541252 | — |
Reaction Steps
In this case, the yield of N-methyl-2H-3-isoquinolone, with a melting point of 235°-236°C., calculated upon the amount of phenacetyl chloride used, reaches 40- 45%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954771 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-5e7668fad78540e9bfd30094e4c73b92 |
| Source note | uspto-grants-1976_05 |