HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,4-Dimethoxyphenyl)acetyl chloride → HCID 21541254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,4-Dimethoxyphenyl)acetyl chloride | HCID 3604458 | — |
| Reactant | HCID 21541249 | HCID 21541249 | — |
| Product | HCID 21541254 | HCID 21541254 | — |
Reaction Steps
Taking into account that the homoveratric acid chloride is obtained with a yield of 83%, the overall yield of 6,7-dimethoxy-N-methyl-2H-3-isoquinolone sulfate, in 3 steps, is 32%, which constitutes a considerable improvement as compared to the process of N. J. Mc Corkindale and A. W. Mc Culloch (4 steps and an overall yield of 13.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954771 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-4e3008d8ba564059ae49c0307b86414a |
| Source note | uspto-grants-1976_05 |