HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12367739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 12367726 | HCID 12367726 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12367739 | HCID 12367739 | — |
Reaction Steps
To a mixture of 1.0 g of 2,3,6,9-tetrahydro-6-hydroxy-2,9-dioxothiazolo[5,4-f]quinoline-8-carboxylic acid, 0.96 g of an 85% -- potassium hydroxide aqueous solution, 20 ml of water and 7 ml of methanol was added dropwise 2.77 g of benzyl bromide and the mixture was stirred for 44 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954775 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-97a4e993dbec4ed99788e425b6117cbd |
| Source note | uspto-grants-1976_05 |