Hydrazine hydrate (1:1) → HCID 12582745, compound

Participants

Reaction Steps

11.7 g of 3-chloro-5,6,7,8,9,10-hexahydrocycloocta[c]pyridazine and 60 cc of hydrazine hydrate are reacted in accordance with the process described in Example 1. The orange-coloured solution is completely concentrated, and the remaining crystalline crude title compound is washed with water. M.P. 145°-148° (decomp., from absolute ethanol).

Provenance & Evidence