HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoyl chloride → HCID 12582692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Reactant | HCID 20441606 | HCID 20441606 | — |
| Reactant | HCID 86733381 | HCID 86733381 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12582692 | HCID 12582692 | — |
Reaction Steps
The 3-chloro-5,6,7,8-tetrahydro-6-(3-phenylpropionyl)pyrido[4,3-c]pyridazine, required as starting material, may be obtained in a manner analogous to that described in Example 8 (g), from 28.6 g of 3-chloro-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine maleate and 31.5 g of 3-phenylpropionyl chloride. M.P. 134°-137° from 95% ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954754 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-b50c6dc5218d4d9292a1d02c01f59b91 |
| Source note | uspto-grants-1976_05 |