HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 20441613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | HCID 12582653 | HCID 12582653 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Product | HCID 20441613 | HCID 20441613 | — |
Reaction Steps
A solution of 5.8 g of 6-cyclobutanecarbonyl-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 50 cc of acetone and 2 drops of glacial acetic acid is heated at reflux on a water bath for 30 minutes. The crude product obtained as a brown oil is crystallized with absolute ethanol. The title compound has a M.P. of 175°-178° (decomp., from acetone/ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954754 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-25e3ddd67f6f48bcb44ff6510e70075e |
| Source note | uspto-grants-1976_05 |