HCID 12582685, compound → HCID 70509251, compound

HRID 1075947Notes

Reaction equation

HRID 1075947 reaction equation
[NH:1]([C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][N:11]([C:13](=[O:26])[C:14]3[CH:19]=[CH:18][C:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)=[CH:16][CH:15]=3)[CH2:12][C:5]=2[CH:4]=1)[NH2:2]>CC(CC)=O>[CH:3](=[N:2][NH:1][C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][N:11]([C:13](=[O:26])[C:14]3[CH:19]=[CH:18][C:17]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)=[CH:16][CH:15]=3)[CH2:12][C:5]=2[CH:4]=1)[CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 1

HCID 12582685HCID 12582685, compound

Product 1

HCID 70509251HCID 70509251, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

0.5 g of 3-hydrazino-6-(p-phenylbenzoyl)-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine are heated in 5 cc of methylethyl ketone on a water bath for 1 hour. The title compound has a M.P. of 260°-262° (decomp., from methylethyl ketone).

Sources & evidence

ORD record
ord-a3900dae991c42908fde60c91bb0cb22
Source dataset
uspto-grants-1976_05
Patent number
US03954754

Reaction notes

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