HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → HCID 20441536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | HCID 12582745 | HCID 12582745 | — |
| Product | HCID 20441536 | HCID 20441536 | — |
Reaction Steps
A solution of 10.0 g of 3-hydrazino-5,6,7,8,9,10-hexahydrocyclooct[c]pyridazine in 100 cc of cyclohexanone is boiled at reflux at a bath temperature of 180° for 1 hour and 45 minutes. The mixture is concentrated in a vacuum, whereby the crystalline title compound is obtained and is recrystallized from isopropanol. M.P. 160°-162° (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03954754 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-c5c89250500141ad8e363671c6ff8848 |
| Source note | uspto-grants-1976_05 |