Gluconic Acid → HCID 131710195, compound

HRID 1076091Notes

Reaction equation

HRID 1076091 reaction equation
[CH3:1][C:2]1[C:6]([CH3:7])=[CH:5][S:4][C:3]=1[CH:8]([OH:14])[CH2:9][NH:10][CH:11]([CH3:13])[CH3:12].[O:15]=[C:16](O)[C@@H:17]([C@H:19]([C@@H:21]([C@@H:23]([CH2:25][OH:26])[OH:24])[OH:22])[OH:20])[OH:18]>O>[O:15]=[C:16]([O:14][CH:8]([C:3]1[S:4][CH:5]=[C:6]([CH3:7])[C:2]=1[CH3:1])[CH2:9][NH:10][CH:11]([CH3:12])[CH3:13])[C@@H:17]([C@H:19]([C@@H:21]([C@@H:23]([CH2:25][OH:26])[OH:24])[OH:22])[OH:20])[OH:18]

Participants

4

Reactant 2

HCID 10690Gluconic AcidHCID 21541773HCID 21541773, compound

Product 1

HCID 131710195HCID 131710195, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent3×

Procedure

To 1.20 g of 1-(3-methyl-4-methylthiophenyl)-2-isopropylaminoethanol in 40 ml of water, 1.96 ml of a 50% gluconic acid solution are added. The mixture is heated in water-bath during 1 hour at 70°, then the solution is lyophilised (2.18 g of the salt obtained are soluble in 5 ml of water and give a pH of 4.6).

Workup

  1. customobtained
  2. customgive a pH of 4.6)

Sources & evidence

ORD record
ord-05cd42bdabc9463a9764f9b75cc3efe1
Source dataset
uspto-grants-1976_05
Patent number
US03954871

Reaction notes

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