Lactic Acid → HCID 131710196, compound

HRID 1076092Notes

Reaction equation

HRID 1076092 reaction equation
[CH3:1][C:2]1[C:6]([CH3:7])=[CH:5][S:4][C:3]=1[CH:8]([OH:14])[CH2:9][NH:10][CH:11]([CH3:13])[CH3:12].[C:15](O)(=[O:19])[CH:16]([CH3:18])[OH:17]>O>[C:15]([O:14][CH:8]([C:3]1[S:4][CH:5]=[C:6]([CH3:7])[C:2]=1[CH3:1])[CH2:9][NH:10][CH:11]([CH3:12])[CH3:13])(=[O:19])[CH:16]([CH3:18])[OH:17]

Participants

4

Reactant 2

HCID 612Lactic AcidHCID 21541773HCID 21541773, compound

Product 1

HCID 131710196HCID 131710196, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

To 1.2 g of 1-(3-methyl-4-methylthiophenyl)-2-isopropylaminoethanol in 32 ml of water, 0.53 g of a 85% aqueous lactic acid solution are added. The product is heated in a water-bath for 2 hours at 50°, then the solution is lyophilised. (1.55g of the salt obtained are soluble in 5 ml of water).

Workup

  1. temperatureThe product is heated in a water-bath for 2 hours at 50°

Sources & evidence

ORD record
ord-6be3001125bb45879af157bc2fc379b2
Source dataset
uspto-grants-1976_05
Patent number
US03954871

Reaction notes

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