化工社化工社 化学情報印刷レポート · 研究参考用
Isobutylene → 1,3,3-Trimethyl-1-phenylindan-5-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutylene | HCID 8255 | — |
| 反応物 | 4-(1-Phenylethyl)phenol | HCID 94763 | — |
| 生成物 | 1,3,3-Trimethyl-1-phenylindan-5-ol | HCID 103816 | 13.5% |
反応手順
112 g of isobutylene were introduced with stirring into 198 g of 1-phenyl-1-(4-hydroxy-phenyl)-ethane and 30 g of an acid activated Fuller's earth at 150°C and the reaction mixture was then stirred at this temperature for 5 hours. 34 g of 1,3,3-trimethyl-1-phenyl-5-hydroxy-indane could be obtained by distillation followed by recrystallisation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03954889 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-9afad045a0df47ec872493d1866cde7b |
| 出典メモ | uspto-grants-1976_05 |