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HRID 1076113作成日:2026年10月25日

Isobutylene → 1,3,3-Trimethyl-1-phenylindan-5-ol

https://huagongshe.com/reaction/1076113

反応式

関与物質

役割名称HCID仕込み量
反応物IsobutyleneHCID 8255—
反応物4-(1-Phenylethyl)phenolHCID 94763—
生成物1,3,3-Trimethyl-1-phenylindan-5-olHCID 10381613.5%

反応手順

112 g of isobutylene were introduced with stirring into 198 g of 1-phenyl-1-(4-hydroxy-phenyl)-ethane and 30 g of an acid activated Fuller's earth at 150°C and the reaction mixture was then stirred at this temperature for 5 hours. 34 g of 1,3,3-trimethyl-1-phenyl-5-hydroxy-indane could be obtained by distillation followed by recrystallisation.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US03954889
出典データセットuspto-grants-1976_05
ORD IDord-9afad045a0df47ec872493d1866cde7b
出典メモuspto-grants-1976_05