Cyclohexanesulfenyl chloride → HCID 11332618, compound

HRID 1076147Notes

Reaction equation

HRID 1076147 reaction equation
C1(SCl)C=CC=CC=1.[CH2:9]([S:19][Cl:20])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]CCC.ClC(SCl)=CCl.C1C2C(=CC=CC=2)C=CC=1SCl.C1(SCl)CCCCC1>>[C:10]1([CH2:9][S:19][Cl:20])[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

6

Reactant 5

HCID 87312Cyclohexanesulfenyl chlorideHCID 11008040Benzenesulfenyl chlorideHCID 124820622-(Chlorosulfanyl)naphthaleneHCID 21983338HCID 21983338, compoundHCID 54122024HCID 54122024, compound

Product 1

HCID 11332618HCID 11332618, compound

Procedure

Similarly, repeating the above procedure but replacing the benzenesulfenyl chloride as used therein with an equal molar proportion of each of decanesulfenyl chloride (prepared by chlorination of decanedisulfide according to the method of Douglass, supra.), 1,2-dichlorovinylsulfenyl chloride, 2-naphthalenesulfenyl chloride, cyclohexanesulfenyl chloride (prepared by chlorination of cyclohexanedisulfide, according to the method of Douglass, supra.) and α-toluenesulfenyl chloride, respectively, there is obtained:

Sources & evidence

ORD record
ord-1d9f9f628582457596cd279bbb1dcb94
Source dataset
uspto-grants-1976_05
Patent number
US03954997

Reaction notes

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