HRID1076180

反应详情

EQUATION

反应方程式

HRID 1076180 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The ethyl ester of 8-methyl-1,2,3,4-tetrahydrocarbazole-1-carboxylic acid is dissolved in cumene and, after adding 10% palladium-carbon, dehydrogenated as set forth in Example 1(b). After recrystallization from methanol, the ethyl ester of 8-methylcarbazole-1-carboxylic acid is obtained in a 75% yield, m.p. 68° C.

WORKUP

后处理

  1. customAfter recrystallization from methanol