4185-98-2 → HCID 21539683, compound
Reaction equation
Cl.[N:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1C(=NO)Cl.Cl.C(=N[OH:22])(Cl)C1C=CN=CC=1.Cl.[C:24](=[N:32][OH:33])(Cl)[C:25]1[CH:30]=[CH:29][CH:28]=NC=1>>[N:2]1[CH:3]=[CH:4][C:5]([C:24]2[CH:25]=[C:30]([CH2:29][CH2:28][OH:22])[O:33][N:32]=2)=[CH:6][CH:7]=1Participants
4
Procedure
By substituting an equimolar amount of picolinoyl chloride oxime hydrochloride or isonicotinoyl chloride oxime hydrochloride for the nicotinoyl chloride oxime hydrochloride employed in the above example, there is obtained the corresponding 3-(2-pyridyl)-5-isozazoleethanol and 3-(4-pyridyl)-5-isoxazoleethanol.
Sources & evidence
- ORD record
- ord-8581c986830c4779ba32ff4a66aa4b15
- Source dataset
- uspto-grants-1976_05
- Patent number
- US03956343
Reaction notes
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