HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 21539628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 5,5-Dimethylhexane-2,4-dione | HCID 81741 | — |
| Product | HCID 21539628 | HCID 21539628 | — |
| Product | HCID 21539664 | HCID 21539664 | — |
Reaction Steps
Similarly, reaction of 5,5-dimethyl-2,4-hexanedione, benzaldehyde and ammonium hydroxide by the procedure of Example 6 with separation of the 1,4-dihydropyridines thus obtained and subsequent treatment with ethyl chloroformate as described above gives 3,5-di-t-butylcarbonyl-1-carbethoxy-1,4-dihydro-2,6-dimethyl-4-phenylpyridine and 3,5-diacetyl-2,6-di-t-butyl-1-carbethoxy-1,4-dihydro-4-phenylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03956341 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-6220eca2044b408cbd59791f6f06fae5 |
| Source note | uspto-grants-1976_05 |