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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1076269Generated: November 2, 2026

Benzaldehyde → HCID 21539628, compound

https://huagongshe.com/reaction/1076269

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantEthyl chloroformateHCID 10928—
ReactantAmmonium HydroxideHCID 14923—
Reactant5,5-Dimethylhexane-2,4-dioneHCID 81741—
ProductHCID 21539628HCID 21539628—
ProductHCID 21539664HCID 21539664—

Reaction Steps

Similarly, reaction of 5,5-dimethyl-2,4-hexanedione, benzaldehyde and ammonium hydroxide by the procedure of Example 6 with separation of the 1,4-dihydropyridines thus obtained and subsequent treatment with ethyl chloroformate as described above gives 3,5-di-t-butylcarbonyl-1-carbethoxy-1,4-dihydro-2,6-dimethyl-4-phenylpyridine and 3,5-diacetyl-2,6-di-t-butyl-1-carbethoxy-1,4-dihydro-4-phenylpyridine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03956341
Source datasetuspto-grants-1976_05
ORD IDord-6220eca2044b408cbd59791f6f06fae5
Source noteuspto-grants-1976_05