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Ethyl glycylglycinate → N-{N-[2-(p-chlorophenoxy)-2-methylpropionyl]glycyl}glycine ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl glycylglycinate | HCID 124706 | — |
| 反応物 | 2,5-Dioxopyrrolidin-1-yl 2-(4-chlorophenoxy)-2-methylpropanoate | HCID 85810950 | — |
| 生成物 | N-{N-[2-(p-chlorophenoxy)-2-methylpropionyl]glycyl}glycine ethyl ester | HCID 21426057 | — |
反応手順
Likewise, by following the procedure of Example 1 but replacing proline methyl ester hydrochloride with glycylglycine ethyl ester and replacing the "activated ester" N-{N-[2-(p-chlorophenoxy)-2-methylpropionyl]glycine} succinimido ester with an equivalent amount of the "activated ester", 2-(p-chlorophenoxy)-2-methyl-propionic acid succinimido ester, obtained in an analogous manner as the aforementioned "activated ester", N-{N-[2-(p-chlorophenoxy)-2-methylpropionyl]glycyl}glycine ethyl ester again is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03956484 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-3bdb08b3e4ee41b3a8453ac327b60bf6 |
| 出典メモ | uspto-grants-1976_05 |