HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl isocyanate → HCID 54204141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl isocyanate | HCID 16035 | — |
| Reactant | Di-n-butyl diacetoxy tin | HCID 9798523 | — |
| Reactant | N-(5-Methyl-1,3-oxathiolan-4-ylidene)hydroxylamine | HCID 71364792 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54204141 | HCID 54204141 | — |
Reaction Steps
4-Oximino-5-methyl-1,3-oxathiolane was caused to react with 2-chloroethylisocyanate in the presence of dibutyltin diacetate in ether. The reaction mixture was worked up and recrystallized in the manner described in Example I. The product had a mp 88.5°-90.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03956500 |
| Source dataset | uspto-grants-1976_05 |
| ORD ID | ord-0850b6880d5c48008bbfe151bded7926 |
| Source note | uspto-grants-1976_05 |