HRID1076411

反应详情

EQUATION

反应方程式

HRID 1076411 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

15.0 g of Z-Asn-Leu-OMe are dissolved in 400 ml of t-butanol-water (9:1) and are hydrogenated in the presence of 2 g of palladium-charcoal (10 %Pd). After completion of the hydrogenation the catalyst is filtered off and the solution evaporated at 40°C. The residue is directly further used.

WORKUP

后处理

  1. filtrationAfter completion of the hydrogenation the catalyst is filtered off
  2. customthe solution evaporated at 40°C