Butyl levulinate → Butyl 4-[2-(2-methylbutan-2-yl)hydrazinylidene]pentanoate

HRID 1076467Notes

Reaction equation

[C:1]([NH:6][NH2:7])([CH2:4][CH3:5])([CH3:3])[CH3:2].[C:8]([O:15][CH2:16][CH2:17][CH2:18][CH3:19])(=[O:14])[CH2:9][CH2:10][C:11]([CH3:13])=O>>[C:1]([NH:6][N:7]=[C:11]([CH3:13])[CH2:10][CH2:9][C:8]([O:15][CH2:16][CH2:17][CH2:18][CH3:19])=[O:14])([CH2:4][CH3:5])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 16331Butyl levulinate

HCID 117546HCID 117546, compound

Product 1

HCID 71364225Butyl 4-[2-(2-methylbutan-2-yl)hydrazinylidene]pentanoateYield 90%

Procedure

Butyl levulinate t-amylhydrazone was prepared in 90% yield by refluxing an aqueous solution of t-amylhydrazine with an equimolar amount of butyl levulinate.

Sources & evidence

ORD record: ord-a0908216c025410189830f3f486afab8
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03957750

Reaction notes

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