Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | Butyl 4-[2-(2-methylbutan-2-yl)hydrazinylidene]pentanoate | HCID 71364225 | — |
| Product | 55296-29-2 | HCID 21412745 | 104% |
Reaction Steps
To a solution of 90 grams (0.316 moles) of butyl levulinate t-amylhydrazone in 150 mls. of petane in a 500 ml. round bottom flask was passed 10.9 grams (.154 moles) of chlorine holding the temperature at -20°C with a dry ice- isopropanol bath. The chlorine was added over 30 minutes and then the reaction was stirred an additional 15 minutes at -20°C and filtered. The filtrate was dried and the pentane evaporated leaving 46.6 grams of crude butyl 4-t-amylazo-4-chlorovalerate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03957750 |
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| Source dataset | uspto-grants-1976_05 |
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| ORD ID | ord-a92a0b0f76454923a4d3a26cf3f77ec9 |
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| Source note | uspto-grants-1976_05 |
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