Chloral → N-Ethyl-N-(2-phenylethyl)formamide

HRID 1076514Notes

Reaction equation

[CH2:1]([NH:3][CH2:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH3:2].[O:12]=[CH:13]C(Cl)(Cl)Cl>>[CH2:1]([N:3]([CH2:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH:13]=[O:12])[CH3:2]

Participants

Reactant 2

HCID 6407Chloral

HCID 547324N-Ethyl-2-phenylethanamine

Product 1

HCID 15041416N-Ethyl-N-(2-phenylethyl)formamide

Procedure

N-Ethyl-N-phenethylformamide was prepared from N-ethylphenethylamine and chloral. The boiling point was 107°-108°C/0.4 mm Hg.

Sources & evidence

ORD record: ord-d9901a7605d14b58870419e34f1afe16
Source dataset: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03957764

Reaction notes

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